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Combustion analysis of C,H,and S converts each element into nonmetal oxide for analysis.Combustion analysis of O requires a different approach.Which of the steps below is(are) not required or false for combustion analysis for O?
I Sample is thermally heated to decompose the compound in the absence of O2.
II Gaseous products from pyrolysis are passed through nickelized carbon at 1 075 oC to convert oxygen into CO.
III Gaseous products are sent to GC for analysis.
IV Halogens are converted to HX during pyrolysis,dissolved in water and titrated with silver nitrate.
V Gaseous products from pyrolysis are passed through nickelized carbon at 1 075 oC to convert oxygen to CO2.
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